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ID 60784
FullText URL
Author
Mitsudo, Koichi Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University ORCID Kaken ID publons researchmap
Habara, Nanae Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Kobashi, Yoshiak Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Kurimoto, Yuji Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Mandai, Hiroki Department of Pharmacy, Faculty of Pharmacy, Gifu University of Medical Science ORCID Kaken ID publons researchmap
Suga, Seiji Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Abstract
A one-pot procedure for the synthesis of thienyl thioethers is described. Several thienyl thioethers were synthesized by a TfOH-promoted Friedel–Crafts-type cyclization, a subsequent nucleophilic attack by an arenethiol, and dehydration. This protocol was successfully applied to the synthesis of thienoacene derivatives by using a Pd-catalyzed dehydrogenative cyclization.
Keywords
thienyl thioethers
thioetherification
one-pot synthesis
metal-free
halide-free
thienoacenes
Note
This is an Accepted Manuscript of an article published by Thieme Gruppe.
Published Date
2020-09-21
Publication Title
Synlett: Accounts and Rapid Communications in Synthetic Organic Chemistry
Volume
volume31
Issue
issue19
Publisher
Thieme Gruppe
Start Page
1947
End Page
1952
ISSN
0936-5214
NCID
AA10731110
Content Type
Journal Article
language
English
OAI-PMH Set
岡山大学
File Version
author
DOI
Web of Science KeyUT
Related Url
isVersionOf https://www.doi.org/10.1055/s-0040-1707280
Funder Name
Japan Society for the Promotion of Science
助成番号
JP16K05695
JP16K05777
JP19K05477
JP19K05478
JP18H04455