ID | 60784 |
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Author |
Mitsudo, Koichi
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
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Habara, Nanae
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Kobashi, Yoshiak
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Kurimoto, Yuji
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Mandai, Hiroki
Department of Pharmacy, Faculty of Pharmacy, Gifu University of Medical Science
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Suga, Seiji
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
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Abstract | A one-pot procedure for the synthesis of thienyl thioethers is described. Several thienyl thioethers were synthesized by a TfOH-promoted Friedel–Crafts-type cyclization, a subsequent nucleophilic attack by an arenethiol, and dehydration. This protocol was successfully applied to the synthesis of thienoacene derivatives by using a Pd-catalyzed dehydrogenative cyclization.
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Keywords | thienyl thioethers
thioetherification
one-pot synthesis
metal-free
halide-free
thienoacenes
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Note | This is an Accepted Manuscript of an article published by Thieme Gruppe.
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Published Date | 2020-09-21
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Publication Title |
Synlett: Accounts and Rapid Communications in Synthetic Organic Chemistry
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Volume | volume31
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Issue | issue19
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Publisher | Thieme Gruppe
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Start Page | 1947
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End Page | 1952
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ISSN | 0936-5214
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NCID | AA10731110
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Content Type |
Journal Article
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language |
English
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OAI-PMH Set |
岡山大学
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File Version | author
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DOI | |
Web of Science KeyUT | |
Related Url | isVersionOf https://www.doi.org/10.1055/s-0040-1707280
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Funder Name |
Japan Society for the Promotion of Science
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助成番号 | JP16K05695
JP16K05777
JP19K05477
JP19K05478
JP18H04455
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