Memoirs of the Faculty of Engineering, Okayama University
Published by Faculty of Enginerring, Okayama University

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Memoirs of the School of Engineering, Okayama University

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Amorphous Oxides Prepared from Organometallic Compounds Part 1. Preparation of Sodium Borosilicate Gels

Miura, Yoshinari
Yuasa Motokazu
Takahashi, Katsuaki
Abstract
Sodium borosilicate gels of compositions similar to that of Vycor(R) glass like 80SiO(2).15B(2)O(3).5Na(2)O(wt%) were prepared from hydrolysis and polycondensation of tetraethyl orthosilicate, trimethyl borate, and sodium methylate under the HCl catalysis. Variation of the gelation time is examined as a function of the mixing ratio of the starting materials and the catalyst. The thermal behavior of the gels has been discussed on the basis of their TG and DTA traces.
ISSN
0475-0071
NCID
AA10699856