JaLCDOI | 10.18926/11773 |
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フルテキストURL | 001_069_076.pdf |
著者 | Sasaki Kenji| Hirota Takashi| Iwado Akimasa| Hirota Kazuhiro| |
抄録 | Reactions of cyclic ketones such as α-tetralone, 1,3-cyclohexanedione, or naphthalenedione with formamide or trisformylaminomethane (TFAM) have shown to form polyclic fused pyrimidines by us. Reactions of terpene ketones like l-menthone, d-camphor, l-carvone with TFAM were performed, and 8-isopropyl-5-methyl-5,6,7,8-tetrahydroquinazoline, borno[2,3-d] pyrimidine, and 5-isopropenyl-8-methyl-5,6-dihydroquinazoline were expectedly obtained from three terpenes. Minor products of 5-isopropenyl-8-methyl-5,6,7,8-tetrahydroquinazoline and 5-isopropenyl-8-methylquinazoline were formed with 5-isopropenyl-8-methyl-5,6-dihydroquinazoline by disproportionation reaction of l-carvone. Furthermore, No-formylmenthylamine, N-formylbornylamine, and N-formylcarvylamine were obtained as the Leuckart-type products terpene ketones in these reactions. The reaction of N-benzyl-4-piperidone with TFAM gave desired 6-benzyl-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine. The reaction of diethyl succinylsuccinate with TFAM afforded tricyclic 4,9-dioxo-3,4,8,9-tetrahydropyrimido[4,5-g]quinazoline. Above compounds were determined by the measurements of their instrumental analyses. |
キーワード | Cyclic ketone Trisformylaminomethane Fused pyrimidine Cyclization Reductive amination |
出版物タイトル | 岡山大学医療技術短期大学部紀要 |
発行日 | 1991-03-25 |
巻 | 1巻 |
開始ページ | 69 |
終了ページ | 76 |
ISSN | 0917-4494 |
言語 | 英語 |
論文のバージョン | publisher |
NAID | 120002313993 |
著者 | 岩藤 章正| |
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発行日 | 1994-03-25 |
出版物タイトル | |
資料タイプ | 学位論文 |
著者 | 岩藤 章正| 椋野 貴| 秋澤 宏行| 御舩 正樹| 齋藤 寛| |
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発行日 | 1998-08 |
出版物タイトル | 環境制御 |
巻 | 20巻 |
資料タイプ | 紀要論文 |
フルテキストURL | fulltext.pdf |
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著者 | Liu, Qingping| Kobayashi, Kazuko| Furukawa, Jun-ichi| Inagaki, Junko| Sakairi, Nobuo| Iwado, Akimasa| Yasuda, Tatsuji| Koike, Takao| Voelker, Dennis R.| Matsuura, Eiji| |
キーワード | antiphospholipid syndrome atherosclerosis autoantibody beta(2)-glycoprotein I oxidized LDL omega-oxidation |
発行日 | 2002-09 |
出版物タイトル | Journal Of Lipid Research |
巻 | 43巻 |
号 | 9号 |
出版者 | Elsevier |
開始ページ | 1486 |
終了ページ | 1495 |
ISSN | 0022-2275 |
NCID | AA00701215 |
資料タイプ | 学術雑誌論文 |
言語 | 英語 |
OAI-PMH Set | 岡山大学 |
著作権者 | © 2002 by Lipid Research, Inc. |
論文のバージョン | publisher |
PubMed ID | 12235181 |
DOI | 10.1194/jlr.M20063-JLR200 |
Web of Science KeyUT | 000178252900016 |
関連URL | isVersionOf https://doi.org/10.1194/jlr.M20063-JLR200 |