| ID | 60783 |
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| Author |
Mitsudo, Koichi
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
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Matsuo, Ren
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Yonezawa, Toki
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Inoue, Haruka
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
Mandai, Hiroki
Department of Medical Technology, Gifu University of Medical Science
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Suga, Seiji
Division of Applied Chemistry, Graduate School of Natural Science and Technology, Okayama University
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| Abstract | The first electrochemical dehydrogenative C−S bond formation leading to thienoacene derivatives is described. Several thienoacene derivatives were synthesized by dehydrogenative C−H/S−H coupling. The addition of nBu4NBr, which catalytically promoted the reaction as a halogen mediator, was essential.
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| Keywords | cross-coupling
cyclization
electrochemistry
heterocycles
synthetic methods
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| Note | This is the peer reviewed version of the following article: Mitsudo Koichi et. al. Electrochemical Synthesis of Thienoacene Derivatives: Transition‐Metal‐Free Dehydrogenative C−S Coupling Promoted by a Halogen Mediator. Angewandte Chemie International Edition 59(20) 7803-7807(2020), which has been published in final form at https://doi.org/10.1002/anie.202001149. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Use of Self-Archived Versions
This fulltext is available in Feb. 2021.
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| Published Date | 2020-02-20
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| Publication Title |
Angewandte Chemie International Edition
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| Volume | volume59
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| Issue | issue20
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| Publisher | Wiley
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| Start Page | 7803
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| End Page | 7807
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| ISSN | 1433-7851
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| NCID | AA11614189
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| Content Type |
Journal Article
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| language |
English
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| OAI-PMH Set |
岡山大学
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| File Version | author
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| Related Url | isVersionOf https://doi.org/10.1002/anie.202001149
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| Funder Name |
Japan Society for the Promotion of Science
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| 助成番号 | JP19K05477
JP19K05478
JP18H04455
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