Memoirs of the Faculty of Engineering, Okayama University
Published by Faculty of Enginerring, Okayama University

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Memoirs of the School of Engineering, Okayama University

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SAXS Intensity Measurements by Photographic Methods

Yamada, Masuo
Sakakibara, Akira
Ohta, Mutsuo
Abstract
Photographic method for measurement of small-angl X-ray scattering (SAXS) is improved. Intense pointfocussing incident beam is obtained by using doubly bent crystal monochromator made of aluminium single crystal. Microphotometry and the subsequent calculation to obtain profiles, Guinier and Porod radii, integrated intensities, and so on are facilitated by using microcomputer. Integrated SAXS intensities measured from an Al-Zn alloy which has been treated under the same heat treatment conditions are coincident with one another with probable errors less than ±6 % . Ratio of the integrated intensities obtained from two Al-Zn alloys of different composition is reasonable compared with the quasi-equilibrium phase diagram.
ISSN
0475-0071
NCID
AA00733903